ASTM C1259-14

1.1 This test method covers determination of the dynamic elastic properties of advanced ceramics at ambient temperatures. Specimens of these materials possess specific mechanical resonant frequencies that are determined by the elastic modulus, mass, and geometry of the test specimen. The dynamic elastic properties of a material can therefore be computed if the geometry, mass, and mechanical resonant frequencies of a suitable (rectangular, cylindrical, or disc geometry) test specimen of that material can be measured. Dynamic Young's modulus is determined using the resonant frequency in the flexural mode of vibration. The dynamic shear modulus, or modulus of rigidity, is found using torsional resonant vibrations. Dynamic Young's modulus and dynamic shear modulus are used to compute Poisson's ratio.

1.2 This test method measures the fundamental resonant frequency of test specimens of suitable geometry by exciting them mechanically by a singular elastic strike with an impulse tool. Specimen supports, impulse locations, and signal pick-up points are selected to induce and measure specific modes of the transient vibrations. A transducer (for example, contact accelerometer or non-contacting microphone) senses the resulting mechanical vibrations of the specimen and transforms them into electric signals. (See Fig. 1.) The transient signals are analyzed, and the fundamental resonant frequency is isolated and measured by the signal analyzer, which provides a numerical reading that is (or is proportional to) either the frequency or the period of the specimen vibration. The appropriate fundamental resonant frequencies, dimensions, and mass of the specimen are used to calculate dynamic Young's modulus, dynamic shear modulus, and Poisson's ratio.

FIG. 1 Block Diagram of Typical Test Apparatus

1.3 Although not specifically described herein, this test method can also be performed at cryogenic and high temperatures with suitable equipment modifications and appropriate modifications to the calculations to compensate for thermal expansion, in accordance with sections 9.2, 9.3, and 10.4 of C1198.

1.4 Where possible, the procedures, sample specifications, and calculations in this test method are consistent with Test Methods C623, C747, C848, and C1198.

1.5 This test method uses test specimens in bar, rod, and disc geometries. The rod and bar geometries are described in the main body. The disc geometry is addressed in Annex A1.

1.6 A modification of this test method can be used for quality control and nondestructive evaluation, using changes in resonant frequency to detect variations in specimen geometry and mass and internal flaws in the specimen. (See 5.5).

1.7 The values stated in SI units are to be regarded as the standard.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.