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ASTM International, 06/01/2016
Publisher: ASTM
File Format: PDF
$34.00$69.00
Published:01/06/2016
Pages:27
File Size:1 file , 430 KB
Note:This product is unavailable in Russia, Ukraine, Belarus
1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade mixed oxides, (U, Pu)O2, powders and pellets to determine compliance with specifications.
1.2 The analytical procedures appear in the following order:
Sections
Uranium in the Presence of Pu by Potentiometric Titration
2
Plutonium by Controlled-Potential Coulometry
Plutonium by Amperometric Titration with Iron (II)
Nitrogen by Distillation Spectrophotometry Using Nessler Reagent
8 to 15
Carbon (Total) by Direct Combustion-Thermal Conductivity
16 to 26
Total Chlorine and Fluorine by Pyrohydrolysis
27 to 34
Sulfur by Distillation-Spectrophotometry
35 to 43
Moisture by the Coulometric, Electrolytic Moisture Analyzer
44 to 51
Isotopic Composition by Mass Spectrometry
3
Rare Earths by Copper Spark Spectroscopy
52 to 59
Trace Impurities by Carrier Distillation Spectroscopy
60 to 68
Impurities by Spark-Source Mass Spectrography
69 to 75
Total Gas in Reactor-Grade Mixed Dioxide Pellets
4
Tungsten by Dithiol-Spectrophotometry
76 to 84
Rare Earth Elements by Spectroscopy
85 to 88
Plutonium-238 Isotopic Abundance by Alpha Spectrometry
5
Americium-241 in Plutonium by Gamma-Ray Spectrometry
Uranium and Plutonium Isotopic Analysis by Mass Spectrometry
89 to 97
Oxygen-to-Metal Atom Ratio by Gravimetry
98 to 105
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safety precaution statements, see Sections 6, 13.2.5, 41.7, and 93.6.1.)
Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
$29.00 $58.00
Standard Test Method for Measurement of Retroreflective Signs Using a Portable Retroreflectometer
Standard Specification for Magnetic Particle Examination of Continuous Grain Flow Crankshaft Forgings
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Standard Test Method for Determination of Titanium Treatment Weight on Metal Substrates by Wavelength Dispersive X-Ray Fluorescence