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ASTM International, 09/01/2018
Publisher: ASTM
File Format: PDF
$24.00$48.00
Published:01/09/2018
Pages:9
File Size:1 file , 150 KB
Note:This product is unavailable in Russia, Ukraine, Belarus
1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium metal to determine compliance with specifications.
1.2 The analytical procedures appear in the following order:
Sections
Dissolution Procedure
2
Plutonium by Controlled-Potential Coulometry
3
Plutonium by Amperometric Titration with Iron (II)
Plutonium by Ceric Sulfate Titration Test Method
Plutonium by Diode Array Spectrophotometry
Uranium by Arsenazo I Spectrophotometric Test Method
8 - 10
Thorium by Thorin Spectrophotometric Test Method
11 - 13
Iron by 1,10-Phenanthroline Spectrophotometric Test Method
14 - 16
Iron by 2,2ʹ-Bipyridyl Spectrophotometric Test Method
17 - 23
Impurities by ICP-AES
Chloride by the Thiocyanate Spectrophotometric Test Method
24 - 26
Fluoride by Distillation-Spectrophotometric Test Method
27-28
Nitrogen by Distillation-Nessler Reagent Spectrophotometric Test Method
29-30
Carbon by the Direct Combustion-Thermal Conductivity Test Method
31 - 33
Sulfur by Distillation-Spectrophotometric Test Method
34 - 36
Isotopic Composition by Mass Spectrometry
37 and 38
Plutonium-238 Isotopic Abundance by Alpha Spectrometry
Americium-241 by Extraction and Gamma Counting
39 - 41
Americium-241 by Gamma Counting
Gamma-Emitting Fission Products, Uranium, and Thorium by Gamma-Ray Spectroscopy
42 - 49
Rare Earths by Copper Spark Spectrochemical Test Method
50 - 52
Tungsten, Niobium (Columbium), and Tantalum by Spectro- chemical Test Method
53 - 55
Sample Preparation for Spectrographic Analysis for Trace Impuri- ties
56 - 60
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