• ASTM C758-18

ASTM C758-18

Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal

ASTM International, 09/01/2018

Publisher: ASTM

File Format: PDF

$24.00$48.00


Published:01/09/2018

Pages:9

File Size:1 file , 150 KB

Note:This product is unavailable in Russia, Ukraine, Belarus

1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium metal to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

 

Sections

Dissolution Procedure

2

Plutonium by Controlled-Potential Coulometry

3

Plutonium by Amperometric Titration with Iron (II)

2

Plutonium by Ceric Sulfate Titration Test Method

3

Plutonium by Diode Array Spectrophotometry

3

Uranium by Arsenazo I Spectrophotometric Test Method

8 - 10

Thorium by Thorin Spectrophotometric Test Method

11 - 13

Iron by 1,10-Phenanthroline Spectrophotometric Test Method

14 - 16

Iron by 2,2ʹ-Bipyridyl Spectrophotometric Test Method

17 - 23

Impurities by ICP-AES

 

Chloride by the Thiocyanate Spectrophotometric Test Method

24 - 26

Fluoride by Distillation-Spectrophotometric Test Method

27-28

Nitrogen by Distillation-Nessler Reagent Spectrophotometric Test
 Method

29-30

Carbon by the Direct Combustion-Thermal Conductivity Test
 Method

31 - 33

Sulfur by Distillation-Spectrophotometric Test Method

34 - 36

Isotopic Composition by Mass Spectrometry

37 and 38

Plutonium-238 Isotopic Abundance by Alpha Spectrometry

 

Americium-241 by Extraction and Gamma Counting

39 - 41

Americium-241 by Gamma Counting

3

Gamma-Emitting Fission Products, Uranium, and Thorium by
 Gamma-Ray Spectroscopy

42 - 49

Rare Earths by Copper Spark Spectrochemical Test Method

50 - 52

Tungsten, Niobium (Columbium), and Tantalum by Spectro-
 chemical Test Method

53 - 55

Sample Preparation for Spectrographic Analysis for Trace Impuri-
 ties

56 - 60

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