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ASTM International, 06/01/2014
Publisher: ASTM
File Format: PDF
$30.00$60.00
Published:01/06/2014
Pages:5
File Size:1 file , 81 KB
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1.1 This test method covers the analysis for commonly determined trace metals in test specimens of raw and calcined petroleum coke by inductively coupled plasma atomic emission spectroscopy.
1.2 Elements for which this test method is applicable are listed in Table 1. Detection limits, sensitivity, and optimum ranges of the metals will vary with the matrices and model of spectrometer.
Element
Wavelengths, nmA ,B
Concentration Range, mg/kgC
Aluminum
237.313, 256.799, 308.216, 396.152
15-110
Barium
455.403, 493.410
1-65
Calcium
317.933, 393.367, 396.847
10-140
Iron
259.940
40-700
Magnesium
279.079, 279.553
5-50
Manganese
257.610, 294.920
1-7
Nickel
231.604, 241.476, 352.454
3-220
Silicon
212.412, 251.611, 288.159
60-290
Sodium
588.995, 589.3, 589.592
30-160
Titanium
334.941, 337.280
Vanadium
292.402
2-480
Zinc
202.548, 206.200, 213.856
1-20
1.3 This test method is applicable only to samples containing less than one mass % ash.
1.4 Elements present at concentrations above the upper limit of the working ranges can be determined with additional, appropriate dilutions.
1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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