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ASTM International, 05/01/2014
Publisher: ASTM
File Format: PDF
$30.00$60.00
Published:01/05/2014
Pages:9
File Size:1 file , 150 KB
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1.1 This test method covers the determination of selected elements in middle distillate fuels by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1. The concentration range of this test method is approximately 0.1 to 2.0 mg/kg. The test method may be used for concentrations outside of this range; however, the precision statements may not be applicable. Middle distillate fuels covered in this test method have all distillation fractions contained within the boiling range of 150 to 390°C. This includes, but is not limited to, diesel fuels and aviation turbine fuels.
Element
Wavelengths, nm
Aluminum
308.215, 396.153
Barium
455.403, 493.408
Calcium
393.366
Chromium
267.716, 283.563
Cobalt
228.615, 236.375, 238.892
Copper
324.752
Iron
259.939
Lithium
670.784
Lead
224.688, 283.306
Magnesium
279.553
Manganese
257.610
Molybdenum
204.597, 281.616
Nickel
221.648, 341.476
Phosphorus
214.914, 213.618
Palladium
340.458, 342.124
Platinum
214.423
Potassium
766.490
Sodium
588.995
Silicon
251.611
Silver
328.068
Strontium
407.771
Tin
283.999, 189.991
Titanium
334.940
Vanadium
310.230
Zinc
213.857
1.2 This test method is not intended to analyze insoluble particulates. However, very small particulate matter (smaller than a micrometre) will be carried into the plasma and be included in the quantitative analysis.
1.3 This test method may give a result that is higher than the true value if an analyte is present in the sample in a form which is sufficiently volatile. For example, hexamethyldisiloxane will generate a biased high result for silicon.
1.4 The values stated in SI units are to be regarded as standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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